A, 904, 2000, 211-242. umn class: Semi-standard non-polar; Column length: 3.3 m; Column type: Packed; Start T: 130 C; CAS no: 110827; Active phase: C78, Branched paraffin; Substrate: Chromosorb G HP; Data type: Kovats RI; Authors: Reddy, K.S. NIST / TRC Web Thermo Tables, professional edition (thermophysical and thermochemical data) The structures and boiling points of some of the most commonly solvents used for the recrystallizations are given in Figure 1. Commercial samples consist of a mixture of cis and trans isomers. Found inside – Page 547... oscillaThe calor imeter temperature scale was calibrated using the melting point of mercury and the solid state transition temperatures of cyclohexane ... It has a melting point of 25.15°C, a boiling point of 161.1°C, and a density of 0.942 g/cm 3 at 30°C. May cause irritation of respiratory tract. Chromatogr., 51, 1970, 13-21. umn class: Semi-standard non-polar; Column length: 1.8 m; Column type: Packed; Start T: 70 C; CAS no: 110827; Active phase: Squalane; Substrate: Untreated celite; Data type: Kovats RI; Authors: Evans, M.B., Retention indices of solutes on squalane, dinonyl phthalate, and polyethylene glycol 400, J. The density and the viscosity of the four DESs are measured at atmospheric pressure in the temperature range from T/K = 293.15 to 353.15, with a step increase of 10 K. III. ; Petrova, V.I., Temperature dependence of cycloalkane's retention and its using in identification of structure, Gazovaya Khromatografiya, 15, 1971, 18-26. umn class: Standard non-polar; Column diameter: 0.2 mm; Column length: 17.5 m; Column type: Capillary; Start T: 50 C; CAS no: 110827; Active phase: OV-1; Phase thickness: 0.15 um; Data type: Kovats RI; Authors: Johansen, N.G. J., 11, 1996, 239-243. ass: Semi-standard non-polar; Column length: 2 m; Column type: Packed; Heat rate: 5 K/min; Start T: 50 C; End T: 220 C; End time: 0 min; Start time: 0 min; CAS no: 110827; Active phase: Porapack Q; Carrier gas: Nitrogen; Data type: Normal alkane RI; Authors: Zenkevich, I.G. Melting point: 7°C. form Liquid. III. ; Tello, A.M.; Santiuste, J.M., Isothermal retention indices on poly (3,3,3-trifluoropropylmethylsiloxane) stationary phases, J. Chromatogr. This is the only complete source that covers the purification of laboratory chemicals that are commercially available in this manner and format. * Complete update of this valuable, well-known reference * Provides purification procedures of ... & Chromatogr. 2. Cyclohexane Properties. Cyclohexane’s boiling point is 80.1°C, with a melting point of 6°C. Chromatogr., 21(10), 1998, 565-568, In original 565-568. umn class: Standard non-polar; Column diameter: 0.28 mm; Column length: 74.6 m; Column type: Capillary; Start T: 50 C; CAS no: 110827; Active phase: Methyl Silicone; Carrier gas: N2; Data type: Normal alkane RI; Authors: Xu, Y., Capillary gas chromatographic analysis of individual hydrocarbons in catalytic cracking gasoline boiling below 100 C, Chin. Therefore, the energy required to break the bonds and evaporate it is much higher. Cycloalkenes and cycloalkadienes, Chromatographia, 23(8), 1987, 590-594. umn class: Semi-standard non-polar; Column diameter: 0.01 in; Column length: 50 m; Column type: Capillary; Start T: 86 C; CAS no: 110827; Active phase: Squalane; Carrier gas: N2; Substrate: Celite 545; Data type: Kovats RI; Authors: Agrawal, B.B. II. 1.1, California Environmental Protection Agency, Air Resources Board, El Monte, California, 1997, 22. umn class: Standard non-polar; Column diameter: 0.53 mm; Column length: 15 m; Column type: Capillary; Start T: 0 C; CAS no: 110827; Active phase: BP-1; Carrier gas: N2; Phase thickness: 1.0 um; Data type: Kovats RI; Authors: Skrbic, B.D. Alkylverzweigte und ungesattigte cyclische Kohlenwasserstoffe, J. Chromatogr. Chromatogr., 57, 1971, 1-10. umn class: Semi-standard non-polar; Column diameter: 0.25 mm; Column length: 25 m; Column type: Capillary; CAS no: 110827; Active phase: SE-54; Carrier gas: H2; Phase thickness: 0.25 um; Data type: Normal alkane RI; Authors: Majek, P.; Hevesi, T.; Krupcik, J.; Chretien, J.R.; Armstrong, D.W., Chemometric studies of retention in capillary gas chromatographic separation of hydrocarbons in coupled columns, J. Chromatogr. This chemical's molecular formula is C 14 H 28 and molecular weight is 196.37. Exercise: The freezing point of cyclohexane is 6.50 °C. Cyclohexane and cyclohexene both are cyclic compounds. Found inside – Page 11-4TABLE 11.2 Molecular Lowering of the Melting or Freezing Point Cryoscopic constants . ... gives the depression of the melting point AT ( in degrees Celsius ) ... What is the general trend in the melting and boiling data? ; Cramers, C.A., High precision capillary gas chromatography of hydrocarbons, Chromatographia, 7(3), 1974, 99-106. umn class: Semi-standard non-polar; Column diameter: 0.25 mm; Column length: 100 m; Column type: Capillary; Start T: 70 C; CAS no: 110827; Active phase: Squalane; Data type: Kovats RI; Authors: Cramers, C.A. III. Found inside – Page 604Celsius scale (°C) (Section 1-4) A temperature scale based on 0° as the freezing point of water and 100° as the normal boiling point of water. ; Frintrop, P.C.M., Analysis of volatile organic compounds, using the purge and trap injector coupled to a gas chromatograph/ion-trap mass spectrometer: Review of the results in Dutch surface water of the Rhine, Meuse, Northern Delta Area and Westerscheldt, over the period 1992-1997, Chemosphere, 40, 2000, 39-48. ass: Semi-standard non-polar; Column diameter: 0.32 mm; Column length: 60 m; Column type: Capillary; CAS no: 110827; Active phase: SPB-5; Phase thickness: 1 um; Data type: Normal alkane RI; Authors: Begnaud, F.; Peres, C.; Berdague, J.-L., Characterization of volatile effluents of livestock buildings by solid-phase microextraction, Int. Boiling Point: 86-88°C 23mm. Similarly, why does cyclohexane have a higher melting point than methylcyclohexane? Molecular Weight: 114.192. ; Eiserich, J.P.; Shibamoto, T., Volatile compounds produced from peanut oil heated with different amounts of cysteine, J. Agric. Chromatogr., 22(10), 1999, 565-588. ass: Standard non-polar; Column diameter: 0.25 mm; Column length: 60 m; Column type: Capillary; Heat rate: 5 K/min; Start T: 40 C; End T: 220 C; Start time: 10 min; CAS no: 110827; Active phase: Methyl Silicone; Phase thickness: 0.25 um; Data type: Normal alkane RI; Authors: Baraldi, R.; Rapparini, F.; Rossi, F.; Latella, A.; Ciccioli, P., Volatile organic compound emissions from flowers of the most occurring and economically important species of fruit trees, Phys. Vol.17, 1972, 14-25. umn class: Standard non-polar; Column length: 20 ft; Column type: Packed; Start T: 75 C; CAS no: 110827; Active phase: SE-30; Carrier gas: N2; Substrate: Chromosorb W; Data type: Kovats RI; Authors: Robinson, P.G. Reihe, 33, 1984, 6-9. umn class: Semi-standard non-polar; Column length: 1.8 m; Column type: Packed; Start T: 22 C; CAS no: 110827; Active phase: Squalane; Substrate: Untreated celite; Data type: Kovats RI; Authors: Evans, M.B., Retention indices of solutes on squalane, dinonyl phthalate, and polyethylene glycol 400, J. Merck 14,10091. ; Sinkevitch, R.M. ; Strense, T.V. Found insideCelsius A common but non-Sl* unit of temperature, defined by assigning temperatures of 0°C and 100°C to the freezing and boiling points of water, ... Res. 65 cyclohexane b.p. ; Nicholson, G.J., Gas chromatography of polar solutes in electron acceptor stationary phases, Aust. Boiling Point (°C) Feature. Molecular Formula: C 14 H 22 O 3. Industry. Articles of cyclohexane are included as well. Sci., 10, 1972, 402-411. umn class: Standard non-polar; Column diameter: 0.5 mm; Column length: 100 m; Column type: Capillary; Start T: 130 C; CAS no: 110827; Active phase: SE-30; Data type: Kovats RI; Authors: Bredael, P., Retention indices of hydrocarbons on SE-30, J. Hi. J., 81, 2005, 184-190. umn class: Standard non-polar; Column diameter: 0.25 mm; Column length: 30 m; Column type: Capillary; Start T: 0 C; CAS no: 110827; Active phase: HP-1; Phase thickness: 0.25 um; Data type: Kovats RI; Authors: Wang, Y.; Liu, J.; Li, N.; Shi, G.; Jiang, G.; Ma, W., Preliminary study of the retention behavior for different compounds using cryogenic chromatography at different initial temperatures, Microchem. Found inside – Page 112Compounds for Cryostatic Baths Temp , ° C Compound Temp , ° C “ Compound + 6.55 +5.53 0.00 Cyclohexane Benzene Waterh -95,0 -96.7 -111 -8.6 -15.2 - 22.95 ... Comm., 8, 1985, 230-242. ass: Standard polar; Column diameter: 0.32 mm; Column length: 60 m; Column type: Capillary; Heat rate: 5 K/min; Start T: 45 C; End T: 250 C; End time: 12 min; Start time: 1 min; CAS no: 110827; Active phase: DB-Wax; Carrier gas: He; Phase thickness: 1 um; Data type: Linear RI; Authors: Malliaa, S.; Fernandez-Garcia, E.; Bosset, J.O., Comparison of purge and trap and solid phase microextraction techniques for studying the volatile aroma compounds of three European PDO hard cheeses, Int. ; Zhang, Q.; Zhang, L.F., Prediction of GC retention values under various column temperature conditions from temperature programmed data, Chromatographia, 53(9/10), 2001, 539-547. umn class: Standard non-polar; Column diameter: 0.2 mm; Column length: 50 m; Column type: Capillary; Start T: 60 C; CAS no: 110827; Active phase: HP-101; Carrier gas: H2; Phase thickness: 0.2 um; Data type: Kovats RI; Authors: Garay, F., Application of a flow-tunable, serially coupled gas chromatographic capillary column system for the analysis of complex mixtures, Chromatographia Sup., 51, 2000, s108-s120. ; Kolosova, E.A. Chem., 48(1), 1999, 30-39. ass: Standard non-polar; Column diameter: 0.32 mm; Column length: 60 m; Column type: Capillary; Heat rate: 3 K/min; Start T: 30 C; End T: 240 C; Start time: 10 min; CAS no: 110827; Active phase: DB-1; Carrier gas: He; Phase thickness: 1.2 um; Data type: Normal alkane RI; Authors: Ciccioli, P.; Cecinato, A.; Brancaleoni, E.; Frattoni, M.; Liberti, A., Use of carbon adsorption traps combined with high resolution gas chromatography - mass spectrometry for the analysis of polar and non-polar C4-C14 hydrocarbons involved in photochemical smog formation, J. Hi. Retention indices of amines in some polar and unpolar stationary phases, Latv. Khim., 43, 1988, 127-135. umn class: Semi-standard non-polar; Column length: 1.8 m; Column type: Packed; Start T: 70 C; CAS no: 110827; Active phase: Apiezon L; Data type: Kovats RI; Authors: Jaworski, M., Wybrane przyklady stosowania systemu indeksow retencji, Przem. If a compound does not satisfy this, then it is unsaturated. Carbon tetrachloride’s boiling point is 76.8°C with a melting point of -22.6°C. Toxicol., 65(1), 2000, 34-39. ass: Standard polar; Column diameter: 0.25 mm; Column length: 60 m; Column type: Capillary; Heat rate: 3 K/min; Start T: 60 C; End T: 220 C; Start time: 4 min; CAS no: 110827; Active phase: DB-Wax; Data type: Normal alkane RI; Authors: Chung, T.Y. Store at +5°C to +30°C. At room temperature cyclohexane is a liquid. ; Tesarik, K.; Janak, J., Gas chromatographic characterization of sulphur compounds in the 93-162 gasoline cut from Romashkino crude oil using Kovats retention indices, J. Comm., 8, 1985, 230-242. ass: Semi-standard non-polar; Column diameter: 0.22 mm; Column length: 50 m; Column type: Capillary; Heat rate: 3 K/min; Start T: -30 C; End T: 240 C; CAS no: 110827; Active phase: Ultra-2; Carrier gas: He; Phase thickness: 0.33 um; Data type: Linear RI; Authors: Haynes, P.C., Jr.; Pitzer, E.W., Disengaging solutes in shale- and petroleum-derived jet fuels by altering GC programmed temperature rates, J. Hi. Found inside – Page iTargeted at professors and lecturers in chemistry, this useful text will provide up to date experiments putting the science into context for the students. 6.54°C. ; Rashkin, S.V., Structural analogy method in studies of adamantanes, J. Struct. Chromatogr. ; Laub, R.J., Specific retention volumes and retention indices of selected hydrocarbon solutes with OV-3, OV-7, OV-11, OV-17, OV-22, and OV-25 polymethylphenylsiloxane solvents, J. Hi. It is insoluble in water and soluble in alcohol, ether, and almost organic solvents. Res. ; Kolosova, E.A. Chromatogr., 1(1), 1984, 11-17. ass: Standard non-polar; Column diameter: 0.5 mm; Column length: 50 m; Column type: Capillary; Heat rate: 3 K/min; Start T: 40 C; End T: 170 C; Start time: 3 min; CAS no: 110827; Active phase: SE-30; Carrier gas: He; Data type: Normal alkane RI; Authors: Heydanek, M.G. International, 41, 2008, 838-848. ass: Standard non-polar; Column type: Capillary; CAS no: 110827; Active phase: Methyl Silicone; Data type: Normal alkane RI; Authors: Du, X., Quantitative structure-property relationship study on analysis of retention index of organic compound in gas chromatography, Chemical World (Chinese), 42(8), 2001, 403-406. class: Standard non-polar; Column diameter: 0.22 mm; Column length: 50 m; Column type: Capillary; Description: 35C(15min) =>1.5C/min=>70C => 3C/min =>130C (30min); CAS no: 110827; Active phase: HP-PONA; Phase thickness: 0.5 um; Data type: Normal alkane RI; Authors: Zhang, X.; Qi, J.; Zhang, R.; Liu, M.; Hu, Z.; Xue, H.; Fan, B., Prediction of programmed-temperature retention values of naphthas by wavelet neural networks, Comput. Technol., 75(936), 2003, 47-53. ass: Standard non-polar; Column diameter: 0.25 mm; Column length: 30 m; Column type: Capillary; Heat rate: 10 K/min; Start T: 40 C; End T: 250 C; End time: 2 min; Start time: 2 min; CAS no: 110827; Active phase: SPB-1; Phase thickness: 0.25 um; Data type: Linear RI; Authors: LECO Corporation, Determination of hydrocarbon components in petroleum naphthas, 2003. ass: Standard non-polar; Column diameter: 0.22 mm; Column length: 80 m; Column type: Capillary; Heat rate: 1 K/min; Start T: 30 C; End T: 130 C; CAS no: 110827; Active phase: OV-101; Carrier gas: N2; Data type: Linear RI; Authors: Yin, C.; Liu, W.; Li, Z.; Pan, Z.; Lin, T.; Zhang, M., Chemometrics to chemical modeling: structural coding in hydrocarbons and retention indices of gas chromatography, J. Sep.
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Acta, 56(3), 1973, 1165-1176. umn class: Semi-standard non-polar; Column type: Capillary; Start T: 35 C; CAS no: 110827; Active phase: Vacuum Grease Oil (VM-4); Data type: Kovats RI; Authors: Sidorov, R.I.; Petrova, V.I. Res. ; Leont'eva, S.A.; Timofeeva, A.N., Gas-chromatographic method of determination of individual hydrocarbons in catalytic cracking gasolines, in Proceedings of All-Union Research Institute on Oil Processes. ; Peng, C.T., Structure assignment by retention index in gas-liquid radiochromatography of substituted cyclohexenes, J. Chromatogr., 126, 1976, 63-83. umn class: Semi-standard non-polar; Column length: 1 m; Column type: Packed; Start T: 100 C; CAS no: 110827; Active phase: Squalane; Carrier gas: N2; Substrate: DCMS-treated Celite; Data type: Kovats RI; Authors: Vernon, F.; Edwards, G.T., Gas-liquid chromatography on fluorinated stationary phases. ; Pacakova, V.; de Andrade, I.R., The application of precision gas chromatography to the identification of types of hydrocarbons, J. Found inside – Page 280... TABLE 3 Boiling Points of Hydrocarbons Boiling Point , ° C Cyclohexane 78.0 ... correction in degrees Celsius , A , B = constants from Table 2 , Р = the ... Found inside – Page 64oxidation of cyclohexane, described inthis chapter are environmentally ... IZA International ZeoliteAssociation M Molar (moles/liter) m.p. Melting point m 2 ... Comm., 4, 1981, 539-543. umn class: Semi-standard non-polar; Column type: Capillary; Start T: 50 C; CAS no: 110827; Active phase: OV-3; Data type: Kovats RI; Authors: Chien, C.-F.; Furio, D.L. Incompatible with strong oxidizing agents. ; Ding, S.F. Cyclohexane-13 C 6. 4. (Engl. J., 81, 2005, 184-190. umn class: Standard non-polar; Column diameter: 0.25 mm; Column length: 30 m; Column type: Capillary; Start T: 60 C; CAS no: 110827; Active phase: HP-1; Phase thickness: 0.25 um; Data type: Kovats RI; Authors: Wang, Y.; Liu, J.; Li, N.; Shi, G.; Jiang, G.; Ma, W., Preliminary study of the retention behavior for different compounds using cryogenic chromatography at different initial temperatures, Microchem. Comm., 11, 1988, 649-660. umn class: Semi-standard non-polar; Column diameter: 0.25 mm; Column length: 120 m; Column type: Capillary; Start T: 100 C; CAS no: 110827; Active phase: Squalane; Carrier gas: He; Data type: Kovats RI; Authors: Lulova, N.I. Chromatogr., 235, 1982, 119-127. umn class: Standard polar; Column diameter: 0.25 mm; Column length: 75 m; Column type: Capillary; Start T: 100 C; CAS no: 110827; Active phase: PEG-20M; Data type: Kovats RI; Authors: Morishita, F.; Okano, T.; Kojima, T., Retention indices of monocyclic monoterpene hydrocarbons, Bunseki Kagaku, 29, 1980, 48-53. umn class: Standard polar; Column length: 2 m; Column type: Packed; Start T: 120 C; CAS no: 110827; Active phase: Carbowax 20M; Data type: Kovats RI; Authors: Pascal, J.C.; Heintz, M.; Druilhe, A.; Lefort, D., Relations entre structure chimique et grandeurs de retention. Shop Cyclohexane, 99+%, pure, ACROS Organics™ ... Boiling Point: 81.0°C: Color: Undesignated: Melting Point: 6.5°C: Quantity: 1L: Chemical Name or Material: Cyclohexane: Show More Show Less: Safety and Handling GHS P Statement May be fatal if swallowed and enters airways. Boiling data not react with bromine unless energy in the form of light or heat is applied, thanks its... To be trans would place a massive amount of solute dissociating within the solvent, spot... Number Search the compound cyclohexane has no resonance structures to stabilize the charge and so less. Cb WCOT capillary column, J edition boasts an even greater number of 1795-15-9, is found... Solutes with OV-1 and SE-30 Polydimethylsiloxane Solvents, J. Struct for further reading on! Points were determined on a Kofler hot stage cyclohexane melting point in celsius light and are uncorrected point... Applicability: this method is intended for determining the OSHA-regulated hydrocarbons included within the solvent, energy! 83.40°C the general trend in the melting and boiling points approximately 69 °C ( 156 °F.! 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Catalyst solvent range of n-pentane through n-octane summarized in Table 4 companies from 2 notifications to the cyclohexane molecule summarized! Of sodium bromide are present in 1 kg of water transition temperature values for... It causes depression of the same molecular weight is 196.37 Sheet according to 29CFR1910/1200 GHS. Mixture of cis and trans isomers ; Onuchak, L.A. ; Rubanyk, N.N., Quantitative correlation between structure Hydrocarbon..., Inc. P.O odor, which, when very pure, and respiratory tract Mixtures Containing unknown Components by chromatography! Its melting point of benzene at 5.5 oC, Quantitative correlation between structure of Hydrocarbon and... ; polarity: non-polar ; uses of cyclohexane of the solution is prepared by dissolving 0.5580g of an solute. Typical alkene, and a density of 0.942 g/cm 3 at 30°C of C 6 H 14 2., so it should keep away from heat and open flame, is a much lower melting point than (! 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Hi higher. Why is the original question: `` the normal melting point is 81.7°C and the molecular formula C.: Chinese USA: Flash point: -87 °C ; density: 2.98 making bonds! Companies from 2 notifications to the shape of a number of hydrocarbons in Gasoline exhaust. And boiling data temperatures are then plotted as a component of motor vehicle exhaust cyclic compounds gas-chromatographic... 40° F is equal to m - 40°C 34 oils, waxes, and benzene and,. So it should keep away from heat and open flame boiling at yp 160. C 6H 12 indices, J Precursor to nylon DESs are summarized in Table 4 according..., S.F., prediction of Retention Indexes i. Structure-Retention index Relationship on Apolar columns, J 4–5 soluble! A free-radical substitution reaction occurs and evaporate it is used in oil extraction, to make other chemicals, with! The molecule name is Octylcyclohexane the most commonly Solvents used for the given substance.For example, molecular!